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Transactions of the INDIAN CERAMIC SOCIETY   Vol. 54  1995
Joining of Alumina Ceramics to Metal by Solution Metallization Process
SUBRATA DAs*. A. N. TIWARI**, A. R. KuLKARNI**, T. S. SYUNRY*
Pages : 212-216
DOI : 10.1080/0371750X.1995.10804722
Abstract
Ultra high vacuum (UHV) joining between alumina ceramics and metal is the key to the success of many devices used in modern technology. The conventional processes like high-temperature Sintered Metal Powder Process (SMPP) and active metal brazing are capital intensive and are not suitable for custom made items where the requirement of the product is smaU. ln such l:ases, solution metallization is an easy and economic altern&tive. Over a decade we have perfected this method for the fabrication of high-tech UHV device like Linac. Though this process requires only 1050"C vis-a-vis 1500°C for SMPP, performance-wise ceramic to metal seals made by solution metallization are comparable to or in some respect better than those obtained by other established processes. The bond quality is dependent upon several process parameters. A systematic investigation has been performed to find out the etTect of diffet:"ent process parameters like pretreatment of ceramic, paint composition, metallization temperature, time and atmosphere on ultimate bond strength. Bonding mechanism is also discussed with the help of the re1>ults of XRD and microstructural studies.
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